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SOLUTION
STATE SPECTROMETERS:
SOLID
STATE SPECTROMETER: Bruker
360 MHz DMX
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Varian
600 MHz INOVA:
Our newest spectrometer, purchased as part of the NSF
STC, and the only one (so far) with an actively shielded
magnet. Three channels are available with a 20 amp gradient
driver. Emphasis is on polymers, 19F, diffusion, peptides
and proteins. |
Probes: (all 5mm)
- Varian
Triple Resonance with z-gradient, 1H inverse detection with 13C
and 15N on the outer coil
- Varian
Triple Resonance with z-gradient, 1H or 19F inverse detection
with 13C and 15N-31P on the outer coil
- Varian
Double Resonance with z-gradient, broad band (67Zn, 33S, 14N,
109Ag, 15N-31P) with 1H or 19F on the outer coil
- Nalorac
Triple Resonance with z-gradient (full 20A capable), broad band
(15N-31P) with 1H and 19F on the outer coil
- Nalorac
Single Resonance Diffusion with z-gradient (full 20A capable),
1H or 19F detection
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Bruker
500 MHz DRX:
Three channels are available with triple axis, 10 amp gradient
drivers. Emphasis is on polymers, 19F, diffusion, and extended
1H & 13C and variable temperature work. |
Probes:
- Nalorac
5mm Triple Resonance with x,y,z-gradients, 1H inverse detection
with 31P and 109Ag-31P on the outer coil (#73)
- Nalorac
5mm Double Resonance with x,y,z-gradients, 1H or 19F on the inner
coil and 1H or 19F on the outer coil (#74)
- Nalorac
5mm Single Resonance Diffusion with z-gradient, 1H or 19F, (#76)
- Nalorac
5mm Double Resonance with x,y,z-gradients, broad band (15N-31P)
and 1H & 19F on the outer coil (#75)
- Nalorac
3mm Double Resonance with x,y,z-gradients, broad band (15N-31P)
with 1H on the outer coil (#72 )
- Nalorac
3mm Double Resonance with x,y,z-gradient, 1H inverse detection
with 109Ag-31P on the outer coil (#71)
- Bruker
10mm Double Resonance, broad band (109Ag-31P) with 1H on the outer
coil.
- Bruker
4mm Double Resonance LC with z-gradient and 1H and 13C detection.
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Bruker
400 MHz DRX:
Three channels are available with a 10 amp gradient driver.
Emphasis is on walk-up 1H, 13C, 19F, 31P experiments and extended
broad band and variable temperature work. |
Probes: (all 5mm)
- Bruker
Quad Nucleus, 13C and 31P on the inner coil and 1H and 19F on
the outer coil
- Bruker
Dual Resonance, broad band (109Ag-31P) detection with 1H on the
outer coil.
- Bruker
Dual Resonance with z-gradient, broad band (109Ag-31P) detection
with 1H on the outer coil.
- Nalorac
Triple Resonance with z-gradient, 1H inverse detection with 13C
and 15N-31P on the outer coil
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Bruker
400 MHz AVANCE (Single Bay, wide bore):
Two channels are available with a 20 amp gradient driver.
Emphasis is on walk-up 1H, 13C, 31P experiments and diffusion
work (including electrophoretic NMR). |
Probes:
- Nalorac
5mm Four Nucleus with z-gradient, 13C and 31P on the inner coil
and 1H and 19F on the outer coil
- Nalorac
8mm Single Resonance Diffusion with z-gradient, 1H or 19F detection,
external connections for use in electrophoretic NMR
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Bruker
300 MHz AMX (upgraded):
Three channels are available. Emphasis is on walk-up 1H, 13C
and 31P experiments extended 1H, 13C, 31P and variable temperature
work. |
Probes:
- Bruker
5mm Triple Resonance, 13C and 31P detection with 1H on the outer
coil
- Bruker
10mm Double Resonance, broad band (183W-31P) detection with 1H
on the outer coil
- Bruker
5mm Double Resonance, 1H inverse detection with 183W-31P on the
outer coil
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Varian
300 MHz Gemini:
This is our undergraduate NMR which runs samples generated
in synthetic chemistry laboratory courses. Two channels are
available with a sample changer (50 sample). Emphasis is on
1H and 31P. |
Probe:
- Varian
5mm Quad Nucleus probe, 13C and 31P on the inner coil and 1H and
19F on the outer coil
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Bruker
360 MHz DMX (wide bore):
Three high power (1kW) channels are available with a triple
axis 10 amp gradient drivers and a micro imaging cabinet.
Emphasis is on solid state NMR (CPMAS and 2H block decay).
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Solid state NMR probes:
- Bruker
Double Resonance, high power, 4mm CPMAS, with broad band detection
- Bruker
Double Resonance, high power, 7mm CPMAS, with broad band detection
- Bruker
high power, horizontal coil with 1H detection
- Bruker
high power 7mm CRAMPS/MAS with 1H or 19F detection
- Bruker
20mm 2H detection 1H or 19F decouple and 19F lock
- Bruker
Triple Resonance, high power, 4mm CPMAS, with 2 broad band channels
and 1H
High
resolution (liquid state) NMR probe:
- Bruker
Double Resonance, 10mm broad band
- Bruker
5mm, 1H or 19F detection
Micro
imaging probe:
- Bruker
"Micro 2.5", water cooled
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